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纳米压痕仿真 Nanoindentation Simulation

Nanometer indentation test is to obtain the elastic modulus and the critical adhesion friction coefficient of the sample, such as the modulus and the critical adhesion friction coefficient of the sample. Based on its extremely high force and displacement resolution, by continuously recording the extremely high force and displacement resolution of load variation during loading and unloading, nano indentation test is very effective for studying the deformation behavior of material surface at the micro and nano scale.

纳米压痕测试是为了获取小块或薄膜材料样品的弹性模量和压入硬度、薄膜临界附着力摩擦系数等样品的弹性模量和压入硬度、薄膜临界附着力摩擦系数等 参数。基于其极高的力和位移分辨率,通过连续记录加载卸期间极高的力和位移分辨率,纳米压痕测试对研究微纳米尺度下材料表面的变形行为十分有效。

纳米压痕点阵的SEM照片

文献1(2020):Experimental study and crystal plasticity finite element simulations of nano-indentation-induced lattice rotation and the underlying mechanism in TC6 single α-grain(通过实验和晶体塑性有限元模拟研究TC6α相单晶中纳米压痕诱导的晶格旋转及其潜在机理)

Atomic Force Microscopy (AFM) three-dimensional topography of the sample and the simulated height cloud image, it can be seen that the pile-up in the middle of the indentation boundaries is more significant than in the other regions. Extract the surface height of the sample along the axis of the indentation from the simulation result and compare it with the measurement result of the corresponding position of the AFM. As the figure shows, the final indentation depth is 368.3 nm, which is smaller than the previously measured maximum depth of 513 nm. This indicates that after elastic-plastic deformation during the loading process, a 149.7 nm elastic rebound occurs in the subsequent unloading process.

Fig.6. Comparison of: (a) experimental and simulated morphologies of the indentation (b) height along the white arrows across the indentation.

The mapping relationship between the lattice orientations and the IPF colors can be obtained from the IPF map, where the dictionary of Euler angles with the corresponding RGB values is established. A virtual IPF map can then be obtained based on the simulated orientation information and, the lattice orientation is illustrated. A high-resolution lattice orientation map was successfully obtained through PED in the slice beneath the indentation despite the large residual stress caused by severe plastic deformation of the sample, and the experimentally determined IPF map and simulated IPF map are compared in Fig.7.

Fig. 8. IPF map of the slice after indentation: (a) simulation results along X, (b) experimental results along X, (c) experimental results along Z and diffraction patterns obtained from different subgrains, (d) distributions of rotation angles and rotation axes.

Experimental study and crystal plasticity finite element simulations of nano-indentation-induced lattice rotation and the underlying mechanism in TC6 single α-grain

Materials and Design 188 (2020) 108423

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